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In Situ Raman Microscopy Of A Single Graphite Microflake Electrode In A Li(+)-containing Electrolyte

by Nasa Technical Reports Server (ntrs)

2021-01-05 00:14:11

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Highly detailed Raman spectra from a single KS-44 graphite microflake electrode as a function of the applied potential have been collected in situ using a Raman microscope and a sealed spectroelectrochemical cell isolated from the laboratory environ... Read more

Highly detailed Raman spectra from a single KS-44 graphite microflake electrode as a function of the applied potential have been collected in situ using a Raman microscope and a sealed spectroelectrochemical cell isolated from the laboratory environment. Correlations were found between the Raman spectral features and the various Li(+) intercalation stages while recording in real time Raman spectra during a linear potential scan from 0.7 down ca. 0.0V vs Li/Li(+) at a rate of 0.1 mV/s in a 1M LiClO4 solution in a 1: l (by volume) ethylene carbonate (EC): diethyl carbonate (DEC) mixture. In particular, clearly defined isosbestic points were observed for data collected in the potential range where the transition between dilute phase 1 and phase 4 of lithiated graphite is known to occur, i.e. 0.157 Less

Book Details

File size9.69 X 7.44 X 0.05 in
Print pages24
PublisherBiblioGov
Publication date August 7, 2013
LanguageEnglish
ISBN9781289290818
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Nasa Technical Reports Server (ntrs)
Author
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